关键词:
Food additives
Beverages
HPLC
Method validation
BENZOIC-ACID
SOFT DRINKS
CONSUMPTION
POPULATION
SWEETENERS
摘要:
Purpose The purpose of this paper is to determine the level of food additives, caffeine and total sugars in locally manufactured beverages in Mauritius and ascertain their compliance with national and international norms. Design/methodology/approach In total, 48 beverages: 21 soft drinks, 14 ice teas, 5 fruit drinks, 5 nonalcoholic sparkling drinks and 3 tonic waters were analysed for the level of sweeteners (aspartame, acesulfame K and saccharin), preservatives (benzoic and sorbic acid), colours (tartrazine, sunset yellow, quinoline yellow, allura red, amaranth, ponceau 4R, carmoisine, erythrosine, brilliant blue, green S and patent blue), citric acid, caffeine and total sugars. High-performance liquid chromatography methods used to quantify the levels of total sugars, caffeine and additives were validated against parameters such as linearity, recovery, accuracy, precision and limit of quantification. Findings Out of 48 beverages, 13 contained at least one sweetener. The most frequently used sweeteners were acesulfame K and aspartame. Benzoic acid was present in 27 samples (42.32-168.03mg/L). Sorbic acid was present in 14 beverages (13.01-180.38mg/L). Citric acid (0.7-4g/L) was present in all the 48 beverages, while caffeine was present in 20 samples in the range of 14.01-129.42mg/L. Nine samples contained at least one artificial colour and the most frequently used colours were tartrazine, sunset yellow, brilliant blue and carmoisine. The average level of total sugars present in the beverages was 10g/100ml. The validation parameters obtained showed evidence for method suitability. Research limitations/implications Beverages sold by individuals on the street, small restaurants and markets were not analysed. Originality/value This study provides an overview of the chemical composition of soft drinks and their compliance with Food Regulations. It also paves the way to investigate weaknesses, knowledge, attitudes and practices of local manufacturers, which leads to non